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Characterization of Silanol Groups in Protonated Magadiite by 1H and 2H Solid-State Nuclear Magnetic Resonance
1H NMR 2H NMR Hydrogen Bonding Magadiite Silanol Group
2011/12/6
Abstract: Silanol groups in protonated magadiite (H-magadiite) were characterized by 1H and 2H solid-state nuclear magnetic resonance (NMR). H-magadiite and deuterated (D) magadiite were synthesized b...
Effects of Clay Fraction and Temperature on the H2O Self-Diffusivity in Hectorite Gel: A Pulsed-Field-Gradient Spin-Echo Nuclear Magnetic Resonance Study
Complexity of Pore Structure Hectorite H2O NMR Self-Diffusion
2011/12/6
Abstract: Self-diffusion coefficients of H2O molecules in Na-rich hectorite gel were measured by 1H nuclear magnetic resonance (NMR). Spin-echo pulse sequences with magnetic field gradient pulses for ...
A Nuclear Magnetic Resonance (NMR) and Fourier-Transform Infrared (FTIR) Study of Glycine Speciation on a Cd-Rich Montmorillonite
Adsorption Amino Acids Cadmium Glycine Montmorillonite Speciation
2011/12/6
Abstract: As a consequence of treatments with glycine solutions, glycine molecules enter the interlayer of both Ca- and Cd-rich montmorillonite. Measurements of d value suggest that at low glycine con...
Nuclear Magnetic Resonance (NMR) Study of Cd2+ Sorption on Montmorillonite
Adsorption Cadmium Montmorillonite Nuclear Magnetic Resonance
2011/12/8
Abstract: 113Cd solid-state nuclear magnetic resonance (NMR) was used to identify possible Cd2+ adsorption sites in montmorillonite. The montmorillonite was treated with 0.1 and 1 M CdCl2 aqueous solu...
Reactive Al-O-Al sites in a natural zeolite: Triple-quantum oxygen-17 nuclear magnetic resonance
Reactive Al-O-Al sites natural zeolite Triple-quantum oxygen-17 nuclear magnetic resonance
2012/4/1
In framework aluminosilicate materials (e.g., feldspars, zeolites and many others), it is generallyassumed that AlOtetrahedra do not share corners, i.e., that Al-O-Al oxygen sites are avoided whenstoi...
A Synthetic Na-Rich Mica: Synthesis and Characterization by 27Al and 29Si Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
KGa-1 MAS NMR Spectroscopy Metakaolinite Mica Na Mica Synthetic Clay Mineral
2011/12/7
Abstract: A swelling mica, Na2Mg3(Al2Si2)O10F2·xH2O, (hereafter “Na-4 mica”) was synthesized from metakaolinite + MgO and Mg aluminosilicate gels at different temperatures and durations using NaF flux...
Nuclear Magnetic Resonance and X-ray Photoelectron Spectroscopic Investigation of Lithium Migration in Montmorillonite
Lithium Migration Montmorillonite NMR Spectroscopy X-ray Photoelectron Spectroscopy
2011/12/22
Abstract: When Li-saturated montmorillonite is heated to 200?00 癈, the Li ions migrate from interlayer positions to sites in the layer structure. However, the identity of these sites has not been clea...
A 19F Nuclear Magnetic Resonance Study of Natural Clays
27Al Aluminum Clay minerals 19F Fluorine MAS NMR Solid
2011/12/28
A series of natural clays, including 1:1 layer silicates (serpentines, kaolin minerals), smectites, vermiculite, micas, talc, pyrophyllite, sepiolite, and palygorskite, were studied by 19F magic-angle...
13C CPMAS Nuclear Magnetic Resonance Study of the Adsorption of 2-Phenethylamine on Clays
Amine reactions with clays Clay acidic sites Solid state NMR
2011/12/1
Abstract: 2-Phenethylamine 13C-enriched in the beta position was adsorbed on four different aluminum-exchanged days: hectorite, Barasym, Laponite RD, and lithium taeniolite. The sites for adsorption w...
Mechanisms of Palygorskite and Sepiolite Alteration as Deduced from Solid-State 27Al and 29Si Nuclear Magnetic Resonance Spectroscopy
Al coordination Hydrothermal transformation Nuclear magnetic resonance Palygorskite Sepiolite Smectite X-ray powder diffraction
2012/1/6
The mechanisms of palygorskite and sepiolite alteration to smectite under mild hydrothermal conditions were investigated by solid-state 27Al and 29Si magic-angle spinning-nuclear magnetic resonance (M...
Deuterium Nuclear Magnetic Resonance Studies of Water Molecules Restrained by their Proximity to a Clay Surface
Nuclear magnetic resonance Orientation Quadrupolar splitting Smectite Surface acidity Water
2012/1/6
Observation of quadrupolar splittings for 2H and 17O nuclei from D2O solvent molecules in suspensions of the Ecca Gum BP bentonite points unambiguously to the ordering of water molecules with respect ...
Quantification of Crystalline and Noncrystalline Material in Ground Kaolinite by X-ray Powder Diffraction, Infrared, Solid-State Nuclear Magnetic Resonance, and Chemical-Dissolution Analyses
Chemical dissolution Dry grinding Infrared spectroscopy Kaolinite Noncrystalline Nuclear magnetic resonance X-ray powder diffraction
2012/1/5
The capabilities of X-ray powder diffraction (XRD), infrared absorption (IR), solid-state magic-angle-spinning nuclear magnetic resonance (MAS-NMR), and chemical dissolution methods were assessed for ...
Structure and Thermal Transformations of Imogolite Studied by 29Si and 27Al High-Resolution Solid-State Nuclear Magnetic Resonance
Aluminosilicate gel Crystal structure Dehydroxylation Imogolite Nuclear magnetic resonance Thermal treatment X-ray powder diffraction
2012/1/5
Solid-state nuclear magnetic resonance (NMR) spectroscopy, thermal analysis, and X-ray powder diffraction data on the tubular, hydrous aluminosilicate imogolite were found to be fully consistent with ...
Further Consideration of the 29Si Nuclear Magnetic Resonance Spectrum of Kaolinite
Hydrazine Hydrogen bond Kaolinite Nuclear magnetic resonance Stacking fault
2011/11/25
Abstract: The introduction of artificial ±b/3 stacking faults into well-crystallized kaolinite by intercalating and removing hydrazine had no observable effect on the solid-state 29Si nuclear magnetic...
Nuclear Magnetic Resonance, Infrared, and X-ray Powder Diffraction Study of Dimethylsulfoxide and Dimethylselenoxide Intercalates with Kaolinite
Dimethylselenoxide Dimethylsulfoxide Infrared spectroscopy Intercalate Kaolinite Nuclear magnetic resonance X-ray powder diffraction
2012/1/10
Dimethylselenoxide (DMSeO) forms three structurally resolvable intercalates with kaolinite (d(001) = 10.95, 11.26, and 11.38 侌). The 11.26-侌 kaolinite: DMSeO intercalate is structurally analogous to t...